http://dx.doi.org/10.15344/2455-2372/2016/129
Abstract
In this study, the possibility of using colemanite mineral (2CaO.3B2O3.5H2O) which cannot be used directly as an additive for fast firing ceramic bodies due to execution of its crystal water through the micropores, was examined after microwave-assisted calcination. For this purpose, domestic microwave oven which was modified with fiber boards, SiC susceptors and thermocouple setup was used. Colemanite powders heat-treated in a porcelain crucible under microwave condition with three different power levels of 385, 539 and 700 W. Temperature profiles of samples were defined as a function of time and calcination states were determined by confirming volumetric expansion and weight loss. When findings were systematically evaluated by X-ray diffraction (XRD) and thermal analysis (DTA/TG), surface area (BET), volume expansion analysis, the results were in favor of microwave-assisted calcination than conventional one in terms of efficiency for both time and temperature of heat treatments.